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Publication et brevets

A reusable TNF-tagged chiral bis(oxazoline)-copper catalyst for Diels-Alder transformations D. Didier, E. Schulz, Synlett 2012, 23, 1309-1314.

Electropolymerization of Chiral Chromium Salen Complexes: New Materials for Heterogeneous Asymmetric Catalysis - A. Zulauf,X. Hong, F. Brisset, E. Schulz, M. Mellah, New J. Chem. 2012, 36, 1399-1407.

Electrogenerated polymers as efficient and robust heterogeneous catalysts for the hydrolytic kinetic resolution of terminal epoxides - X. Hong,M. Mellah,F. Bordier,R. Guillot, E. Schulz, ChemCatChem. 2012, DOI : 10.1002/cctc.201200085.

Ultrasound and Microwaves: Recent Advances in Organic Chemistry, Ed. Jean Pierre Bazureau and Micheline Draye, Research Signpost, ISBN : 978-81-7895-532-2  - M. Draye, J. Estager, E. Naffrechoux, J.-M. Lévêque, Organique Sonochemistry, 2012, chapitre 1, p1-34 et chapitre 2, 35-54.

Ultrasound and ionic liquid: an efficient combination to tune the mechanism of alkenes epoxidation, G. Chatel, C. Goux-Henry, N. Kardos, Joël Suptil, B. Andrioletti, M. Draye, Ultrasonics sonochemistry, 2012, 19, 390-394.

Recycling chiral copper-bis(oxazoline) complexes in an original multi-reactions procedure - D. Didier, E. Schulz, ChemCatChem. 2011, 3, 1880-1884.

New Insight into Indium electrochemistry in a Tf2N – based Room-Temperature Ionic Liquid, Y. Traoré, S. Legeai, S. Diliberto, G. Arrachart, S. Pellet-Rostaing, M. Draye, Electrochimica Acta, 2011, 58, 532-540.

Reusable task-specific ionic liquids for a clean e-caprolactam synthesis under mild conditions, R. Turgis, J. Estager, M. Draye, V. Ragaini, W. Bonrath, J.-M. Lévêque, ChemSusChem, 2011, 3, 1403-1408.

Swift and efficient sono-hydrolysis of nitriles to carboxylic acids in basic condition: role of the oxide anion radical in the hydrolysis mechanism, P. Lignier, J. Estager, N. Kardos, L. Gravouil, J. Gazza, E. Naffrechoux, M. Draye, Ultrasonics sonochemistry, 2011, 18, 28–31.

Ligands supportés à haute densité locale d'atomes coordinants, Hierso, J.-C., Beaupérin, M.; Meunier, P., World Patent PCT, 2011

Enantioselective Friedel–Crafts alkylation of indole derivatives catalyzed by new Yb(OTf)3-pyridylalkylamine complexes as chiral Lewis acids. G. Grach, A. Dinut, S. Marque, J. Marrot, R. Gil, D. Prim, Org. Biomol. Chem., 2011, 9, 497-503.

Charge-transfer interactions : an efficient tool for recycling bis(oxazoline)-copper complexes in asymmetric Henry reactions. D. Didier, C. Magnier-Bouvier, E. Schulz, Adv. Synth. Catal. 2011, 353, 1087-1095.

Chiral Ionic Liquids derived from (-)-ephedrine and carbohydrates: Synthesis, Properties and Applications to Asymmetric Synthesis and Catalysis. T. K. T. Truong, O. Nguyen Van Buu, A. Aupoix, B. Pégot, G. Vo-Thanh, Curr. Org. Synth., 2011 (accepted for publication)

Asymmetric transfer hydrogenation of aromatic ketone using rhodium complexes of chiral N-heterocyclic carbenes derived from (S)-pyroglutamic acid. A. Aupoix, C. Bournaud, G. Vo-Thanh, Eur. J. Org. Chem., 2011 (accepted for publication)

Electrosynthesis as a Powerful Method for the Generation of Catalytic Intermediates: Efficient Isolation of a Palladium Aryl Halide Oxidative Addition Product". Zinovyeva, V.A.; Luo, C.; Fournier, S.; Devillers, C. H.; Cattey, H.; Doucet, H.; Hierso, J.-C.; Lucas, D. Chemistry-A European Journal, 2011, 17, 9901-9906.

Direct Arylation of Heteroaromatic Compounds with Congested, Functionalised Aryl Bromides at Low Palladium/Triphosphane Catalyst Loading. Roy, D.; Mom, S.; Lucas, D.; Hierso, J.-C. Chemistry-A European Journal, 2011, 17, 6453-6461.

Highly-Dispersed Palladium-Polypyrrole Nanocomposites Pd@PPy: “in-Water” Synthesis and Application for Catalytic Arylation of Heteroaromatics by Direct C–H Bond Activation. Beaupérin, M.; Job A.; Cattey, H.; Meunier, P.; Hierso, J.-C.* Advanced Functional Materials, 2011, 21, 1064-1075.

Cavity microelectrode for studying manganese dioxide powder as pH sensor, C. Cachet-Vivier, B. Tribollet and V. Vivier, Talanta, 2010, 82, pp555-559

Electrochemical coupling reactions of benzyl halides on a powder cathode and cavity cell,  R. F. M. de Souza, C. A. de Souza, M. C. C. Areias, C. Cachet-Vivier, M. Laurent, R. Barhdadi, E. Léonel, M. Navarro and L. W. Bieber, Electrochimica Acta, 2010, 56, 575.

Palladium supported on polyether-functionalized mesoporous silica. Synthesis and application as catalyst for Heck coupling reaction, Grandsire, A. F., Laborde, C., Lamaty, F., Mehdi, A., Applied Organometallic Chemistry 2010, 24, pp 179-183.

PEG3400–Cu2O–Cs2CO3: an efficient and recyclable microwave-enhanced catalyticsystem for ligand-free Ullmann arylation of indole and benzimidazole, Colacino, E., Villebrun,  L., Martinez, J., Lamaty, F., Tetrahedron 2010, 66, pp 3730-3735.

Water Microemulsions: New Green Solvents for the Production of Adipic Acid, P. Blach, Z. Böstrom, S. Franceschi-Messant, A. Lattes, I.Rico-Lattes, Tetrahedron, 2010, 66, 7124-7128.

Reusable chiral bis(oxazoline)-copper complexes immobilized by donor-acceptor interactions on insoluble organic supports. G. Chollet, D. Didier, E. Schulz, Catal. Commun. 2010, 11, 351-355.

Recoverable chiral salen complexes for asymmetric catalysis : recent progress. A. Zulauf, M. Mellah, X. Hong, E. Schulz, Dalton Trans. 2010, 39, 6911-6935.

New chiral calixsalen chromium complexes, recyclable asymmetric catalysts. A. Zulauf, M. Mellah, E. Schulz, Chem. Eur. J. 2010, 16, 11108-11114.

Synthesis Of Imidazolium And Pyridinium-Based Ionic Liquids and Applications of 1-Alkyl-3-Methylimidazolium Salts as Pre-Catalysts for the Benzoin Condensation Using Solvent-Free Microwave Activation. A. Aupoix, B. Pégot, Giang Vo-Thanh, Tetrahedron, 2010, 66, 1352-1356.

Synthesis of Functionalized Chiral Ammonium, Imidazolium and Pyridinium-based Ionic Liquids derived from (-)-Ephedrine using solvent-free microwave activation. Applications for the Asymmetric Michael Addition. T. K. T. Truong, G. Vo-Thanh, Tetrahedron, 2010, 66, 5277-5282.

New class of chiral ligands derived from isosorbide: first application in asymmetric transfer hydrogenation. D. Huynh-Khanh, H. Ibrahim, M. Toffano, G. Vo-Thanh, Tetrahedron: Asym., 2010, 21, 1542-1548.

A Versatile Palladium/Triphosphane System for Direct Arylation of Heteroarenes with Chloroarenes at Low Catalyst Loading. Roy, D.; Mom, S.; Beaupérin, M.; Doucet, H.; Hierso, J.-C.* Angewandte Chemie International Edition, 2010, 49, 6650-6654.

Copper(I) Iodide Polyphosphine Adducts at Low Loading for Sonogashira Alkynylation of Demanding Halide Substrates: Ligand Exchange Study between Copper and Palladium. Beaupérin, M.; Job A.; Cattey, H.; Royer, S.; Meunier, P.; Hierso, J.-C.* Organometallics, 2010, 29, 2815-2822.

Direct Arylation of Heterocycles: the Performances of Ferrocene-based Polyphosphane Ligands in Palladium-Catalyzed C–H Bond Activation. Roger, J.; Mom, S.; Beaupérin, M.; Royer, S.; Meunier, P.; Ivanov, V.; Doucet, H; Hierso J.-C.* ChemCatChem., 2010, 2, 296-305.

Solvent-free Microwave-assisted Suzuki-Miyaura Coupling Catalyzed by PEPPSI-iPr, Nun, P.,  Martinez, J.,  Lamaty, F., SYNLETT 2009, pp 1761-1764.

Solvent-free Synthesis of Peptides, Declerck, V., Nun, P.,  Martinez, J.,  Lamaty, F., Angew. Chem. Int. Ed. 2009, 48, pp 9318-9321, Angew. Chem. 2009, 48, pp 9482-9485.

A Straightforward Copper-Free Palladium Methodology for the Selective Alkynylation of a Wide Variety of S-, O-, and N-based Mono- and Diheterocyclic Bromides and Chlorides. Saleh, S.; Picquet, M.; Meunier, P.; Hierso, J.-C.*, Tetrahedron, 2009, 65(34), 7146-7150.

Donor Stabilized-Phosphenium Adducts as New Efficient and Immobilizing Ligand in Palladium-Alkynylation and Platinum-Hydrogenation in Ionic Liquids. Saleh, S.; Fayad, E.; Azouri, M.; Hierso, J.-C.*; Andrieu, J.; Picquet, M., Advanced Synthesis and Catalysis, 2009, 351, 1621-1628.

Conformational Control of Metallocene Backbone by Cyclopentadienyl Ring Substitution: a New Concept in Polyphosphane Ligands Evidenced by “Through-Space” Nuclear Spin-Spin Coupling. Application in heteroaromatics arylation by direct C–H activation. Smaliy, R. V.; Beaupérin, M.; Cattey, H.; Meunier, P.; Hierso, J.-C.*; Roger, J.; Doucet, H.; Coppel, Y. Organometallics, 2009, 28, 3152-3160.

New chiral thiophene salen chromium complexes for the asymmetric Henry reaction. A. Zulauf, M. Mellah, E. Schulz, J. Org. Chem. 2009, 74, 2242-2245.

Original use of the same heterogeneous chiral catalyst batch to promote different asymmetric reactions. A. Zulauf, M. Mellah, E. Schulz, Chem. Commun. 2009, 6574-6576.

Synthesis of Novel Chiral Imidazolium-based Ionic Liquids derived from Isosorbide and their Applications in Asymmetric aza Diels-Alder Reaction. O. Nguyen Van Buu, A. Aupoix, Giang Vo-Thanh, Tetrahedron, 2009, 65, 2260-2265

Solvent-Free Synthesis of Alkylthiazolium-based Ionic Liquids and their use as Catalysts in the Intramolecular Stetter Reaction. A. Aupoix, G. Vo-Thanh, Synlett, 2009, 12, 1915-1920.

Chiral ionic liquids derived from isosorbide: synthesis, properties and applications in asymmetric synthesis. O. Nguyen Van Buu, A. Aupoix, N. Doan Thi Hong, G. Vo-Thanh, New J. Chem., 2009, 33, 2060-2072.